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鈻� 鏂逛究寮曞叆——淇濊鐗瑰畾瀹樿兘鍦樼殑鍙嶆噳(y墨ng)鏀剁巼杓冮珮锛�
鈻� 鏄撲簬浣跨敤——鍦ㄦ櫘閫氱殑鍙嶆噳(y墨ng)姊濅欢涓嬬┅(w臎n)瀹�锛屽湪鐗瑰畾鐨勫弽鎳�(y墨ng)姊濅欢涓嬫槗浜庤劔闄�锛�
鈻� 绱斿害楂�——閬垮厤鍥犲畼鑳藉湗鐨勪繚璀疯�屽紩鍏ュ叾浠栭洔璩�(zh矛)锛屽奖闊块�蹭竴姝ョ殑鍙嶆噳(y墨ng)锛�
鈼� 姘ㄥ熀淇濊鍔戝強鐩搁棞(gu膩n)瑭﹀姂
鏈夋鍚堟垚涓敤渚嗗紩鍏ヤ笉鍚岀殑姘ㄥ熀淇濊鍩哄湗鐨勯噸瑕佽│鍔戯紝闅ㄨ憲姘ㄥ熀淇濊鍩虹殑婕旇畩鍙婄櫦(f膩)灞�锛屼篃琛嶇敓鍑哄姛鑳藉悇鐣�銆佸搧绋箒澶氱殑涓嶅悓鐢�(ch菐n)鍝�锛屽苟閬嬬敤浜庡叆閱�(y墨)钘�銆佽泲鐧借唱(zh矛)鍙婂鑲藉悎鎴愩�佺敓鐗╁寲瀛�(xu茅)椋熷搧锛屽寲濡濆搧绛夊绋敘(ch菐n)鍝佺殑鍚堟垚銆�
.bmp)
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淇濊鍩�
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鐢�(ch菐n)鍝佺啊瀵�
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鐢�(ch菐n)鍝佺法铏�
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鐢�(ch菐n)鍝佸悕绋�
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绲�(ji茅)妲�(g貌u)寮�
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鑴繚璀锋柟娉�
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鍌欐敞
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鐑锋哀缇板熀椤�
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鑺愮敳姘х景鍩篊arbobenzyloxy (Cbz)
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CbzCl
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姘敳閰歌姁閰�, 97%, J&KSeal鐡�
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姘寲鍙嶆噳(y墨ng)
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——
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鍙斾竵姘х景鍩�
tert-Butyloxycarbonyl (BOC)
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Boc anhydride
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浜屽彅涓佸熀浜岀⒊閰搁叝, 99%
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楂樻績搴﹀挤閰�锛屽涓夋盁涔欓吀锛岄菇閰哥瓑
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甯哥敤浜庡浐鐩稿鑲藉悎鎴�
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?锛涱嫙?/strong>
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灏嶇敳鑻：閰板熀
Tosyl (Ts)
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Tosyl chloride
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灏嶇敳鑻：閰版隘, 99%
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楂樻績搴﹂吀(濡傛矮婧撮吀锛岀～閰�)浠ュ強寮烽倓鍘熷姂(濡侼a/NH3,钀樺熀閳�)
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——
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鐑峰熀椤�
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鑺愬熀
Benzyl (Bn)
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BnCl
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鑺愬熀姘�, 99%
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姘寲鍙嶆噳(y墨ng)
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——
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鈼� 缇ュ熀淇濊鍩哄強鐩搁棞(gu膩n)瑭﹀姂锛�
缇ュ熀寤ｆ硾瀛樺湪鑸囪ū澶氬湪鍚堟垚涓婂拰鐢熺悊涓婃湁閲嶈鎰忕京鐨勫寲鍚堢墿涓紝濡傛牳鑻�銆佺⒊姘村寲鍚堢墿銆佺斁鏃忓寲鍚堢墿銆佸ぇ鐠�(hu谩n)鍏�(n猫i)閰鍖栧悎鐗�銆佽仛閱�銆佹煇浜涙皑鍩洪吀鐨勫伌(c猫)閺�銆備竴鑸敤浜庣茎鍩轰繚璀烽啔涓昏鏈夌閱�銆佺敳鍩洪啔銆佺儻涓欏熀閱氥�佽姁鍩洪啔銆佺兎姘х敳鍩洪啔銆佺兎宸板熀鐢插熀閱�銆佷笁鐢插熀纭呬箼鍩虹敳鍩洪啔绛�銆�
.bmp)
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淇濊鍩�
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瑭﹀姂
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瑭﹀姂绶ㄨ櫉
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鐢�(ch菐n)鍝佸悕绋�
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绲�(ji茅)妲�(g貌u)寮�
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鑴繚璀锋柟娉�
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鍌欐敞
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纭呴啔
Silyl ether (TMS,TBDMS,TIPS)
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TIPSCl
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涓夌暟涓欏熀姘鐑�, 97%
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閰告垨姘熼洟瀛�锛�
NaF(429323),HF-Py(322858)鎴朒F-NEt3(112923)
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TBDMS淇濊鍩烘噳(y墨ng)鐢ㄤ簬鏍歌嫹锛屽挨鍏舵槸瀵℃牳鑻烽吀鍚堟垚涓殑2'浣嶇殑缇ュ熀淇濊
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鐗规垔閰板熀
Pivaloyl (Piv)
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Pivaloyl chloride
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鏂版垔閰版隘, 99%
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閰革紝鍫挎垨閭勫師鍔�
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杓冨叾浠栭叞鍩轰繚璀峰熀鏇寸偤绌�(w臎n)瀹�
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鍥涙矮鍚″杻閱歍etrahydropyranyl (THP)
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DHP
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3,4-浜屾矮-2H-鍚″杻, 98%
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閰�
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——
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涓夎嫰鐢插熀
Trityl (Tr)
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Triphenylmethyl chloride
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涓夎嫰鍩烘隘鐢茬兎, 99%
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閰告垨姘寲鍙嶆噳(y墨ng)
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濡侼aF锛孴BAF
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涔欐哀涔欏熀閱欵thoxyethyl ethers (EE)
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Ethoxyethylene
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涔欑儻鍩轰箼鍩洪啔, 99%
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灏嶇敳鑻：閰稿悺鍟堕帗楣�(257101)锛�1M 楂樻隘閰告按婧舵恫
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——
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鈼� 閰嶅鍚堟垚瑭﹀姂