澶氳弻闈�銆佸櫥鑿岄潏鍧囧爆鑻苟鍜攽椤炴鑿屽姂锛屾槸涓�椤為珮鏁堜綆姣掋�佸唬璀�銆佸収(n猫i)鍚告�ф鑿屽姂锛岀洰鍓嶅唬娉涙噳(y墨ng)鐢ㄤ簬钄彍銆佹按鏋滅瓑澶氱ó杈�(n贸ng)浣滅墿鐨勭梾瀹抽槻娌�銆傚鑿岄潏鍖栧(xu茅)鎬ц唱(zh矛)绌�(w臎n)瀹�, 鑳介�氶亷钁夌墖鍜岀ó瀛愭徊鍏ユ鐗╁収(n猫i), 鑰愰洦姘存矕娲�, 灏�(du矛)鍝轰钩鍕�(d貌ng)鐗╂湁涓�瀹氱殑姣掓��锛屽父閫氶亷椋熼亾閫�(j矛n)鍏ヤ汉楂斾娇浜轰腑姣�銆傚洜姝�锛屼汉鍊戦鐢ㄧ殑杈�(n贸ng)鐢�(ch菐n)鍝佷腑澶氳弻闈堟畼鐣欓噺鐨勬脯(c猫)瀹氳秺渚嗚秺鍙楀埌閲嶈銆�
鐧鹃潏濞佷綔鐐哄垎鏋愬寲瀛�(xu茅)闋�(l菒ng)鍩熻妤�(y猫)寮曢牁(l菒ng)鑰咃紝鎿佹湁鍏ㄧ悆鍖栧ぇ鍨嬫(bi膩o)婧�(zh菙n)鍝佸韩锛岀敘(ch菐n)鍝佺郴鍒楁秹鍙婅静(n贸ng)钘ャ�佺煶鍖�銆佺挵(hu谩n)澧冦�侀鍝�銆佺劇姗�(j墨)鍜岀厵鑽夌瓑澶氬��(g猫)闋�(l菒ng)鍩�銆傛墍鏈夋(bi膩o)婧�(zh菙n)鍝佸潎鍙函婧愯嚦NIST銆丯VLAP銆丒PA锛屽苟绗﹀悎ISO 34銆両SO 17025浠ュ強ISO 9001 瑾�(r猫n)璀夌殑瑕佹眰锛屾瘡浠芥(bi膩o)婧�(zh菙n)鍝佸潎闄勫付鍘熸壒娆¤唱(zh矛)妾㈠牨(b脿o)鍛�銆佹潗鏂欏畨鍏ㄦ暩(sh霉)鎿�(j霉)鍗�锛岀⒑淇濇函婧愭��锛屽苟涓斿彲浠ョ偤鐢ㄦ埗鎻愪緵灏堟キ(y猫)妯�(bi膩o)妯ｇ殑瀹氬埗鏈嶅嫏(w霉)銆�
鐧鹃潏濞佸弮鑰僑N/T 1753-2006銆婇��(j矛n)鍑哄彛婵冪府鏋滄眮涓櫥鑿岄潏銆佸鑿岄潏娈樼暀閲忔娓�(c猫)鏂规硶銆嬩互鍙婄浉闂�(gu膩n)鏂囩嵒(xi脿n)璩囨枡锛屽垎鍒ラ枊鐧�(f膩)澶氳弻闈堣垏鍣昏弻闈堢殑鍒嗘瀽鏂规硶锛屼繚璀夊垎鏋愮殑绮剧⒑搴︺��
鈻� 澶氳弻闈堟娓�(c猫)鏂规
鍒嗘瀽鏌憋細C18, 250×4.6 mm, 5 μm
娴佸嫊(d貌ng)鐩革細涔欒厛:姘� =25:75
妾㈡脯(c猫)鍣細FLEx 285 nm Em 315 nm锛圙L-7543A FL Detector锛�
娴� 閫� 锛�0.7 mL/min
|
鐢�(ch菐n)鍝佺法铏�(h脿o)
|
鐢�(ch菐n)鍝佸悕绋�
|
鍖呰
|
鐩寗鍍�(ji脿)
|
|
|
澶氳弻闈�
Carbendazim
|
10 mg
|
锟�169
|
|
|
姘樹唬澶氳弻闈圖3
Carbendazim D3
|
10 mg
|
锟�2124
|
|
|
姘樹唬澶氳弻闈圖4
Carbendazim D4
|
10 mg
|
锟�4,320
|
|
|
C18娑茬浉鑹茶瓬鏌�
HPLC column C18 250×4.6 mm 5 μm
|
1 鏀�
|
锟�2,800
|
|
|
涔欒厛
Acetonitrile, 99.9% [HPLC/ACS]
|
4 L
|
锟�400
|
|
|
姘�
Water [HPLC]
|
4 L
|
锟�375
|
鈻� 鍣昏弻闈堟娓�(c猫)鏂规
鍒嗘瀽鏌憋細C18,250×4.6 mm,5 μm
娴佸嫊(d貌ng)鐩革細鐢查唶锛�0. 02 mol/L纾烽吀楣界珐娌栨恫锛坧H 3.5锛�=50:50
妾㈡脯(c猫)鍣細280 nm 锛圖AD Detector锛�
娴� 閫� 锛�0.8 mL/min
|
鐢�(ch菐n)鍝佺法铏�(h脿o)
|
鐢�(ch菐n)鍝佸悕绋�
|
鍖呰
|
鐩寗鍍�(ji脿)
|
|
|
鍣昏弻闈�
Thiabendazole
|
10 mg
|
锟�169
|
|
|
C18娑茬浉鑹茶瓬鏌�
HPLC column C18 250×4.6 mm 5 μm
|
1 鏀�
|
锟�2,800
|
|
|
鐢查唶
Methanol, 99.9% [HPLC/ACS]
|
4 L
|
锟�180
|
|
|
姘�
Water [HPLC]
|
4 L
|
锟�375
|
|
|
纾烽吀浜屾矮閴�
Potassium phosphate monobasic, 99%
|
500 g
|
锟�51
|
|
|
纾烽吀姘簩閴�
Potassium phosphate dibasic, 99%
|
250 g
|
锟�281
|
鈻� 鍏朵粬鐩搁棞(gu膩n)鍒嗘瀽鑰楁潗鐢�(ch菐n)鍝�
|
鐢�(ch菐n)鍝佺法铏�(h脿o)
|
鐢�(ch菐n)鍝佸悕绋�
|
鍖呰
|
鐩寗鍍�(ji脿)
|
|
|
Bond Elut Plexa PCX, 60 mg, 3 mL
|
50 /pk
|
锟�1111
|
|
|
閲濈瓛寮忔烤鑶滈亷婵惧櫒 肖13, 0.2 μm锛堟湁姗�(j墨)鐩革級
|
100 鐗�/鍖�
|
锟�150
|
|
|
寰瓟婵捐啘 肖50, 0.45 μm锛堟湁姗�(j墨)鐩革級
|
100 鐗�/鍖�
|
锟�210
|
|
|
J锛咾 鐡跺彛鍒嗛厤鍣紙5.0-50.0 mL锛�
|
1 鏀�
|
锟�2,000
|
|
|
J锛咾鍠亾鎵嬪嫊(d貌ng)鍙(di脿o)绉绘恫鍣紙100-1000 μL锛�
|
1 鏀�
|
锟�340
|
|
|
J锛咾纾佸姏鏀媽鍣紙鏁�(sh霉)椤�銆佸姞鐔�銆佷笉閵归嫾锛�
|
1 鑷�(t谩i)
|
锟�3,112
|
|
|
铻虹磱閫忔槑妯ｅ搧鐡讹紙钘�(l谩n)鑹茶灪绱嬭搵锛孭TFE绱呰壊纭呮闅斿锛�
|
100 鍊�(g猫)/鍖�
|
锟�527
|
|
|
鑱氫笝鐑灪绱嬬摱钃嬶紙鐒￠殧澧婏級
|
100 鍊�(g猫)/鍖�
|
锟�109
|
|
|
楂樼礆(j铆)缍犺壊闅斿锛堝付闋�(y霉)绌垮瓟锛�
|
50 鍊�(g猫)/鍖�
|
锟�699
|
|
|
1.5 mL妯�(bi膩o)婧�(zh菙n)姣涚窗(x矛)鍎�(ch菙)瀛樼摱
|
1 鍊�(g猫)
|
锟�240
|