琛嶇敓鍖栨妧琛�(sh霉)鏄寚灏囬洠浠ユ娓殑鐩(bi膩o)鍖栧悎鐗╁畾閲忚綁(zhu菐n)鍖栨垚鍙︿竴绋槗浜庡垎鏋愭娓殑鍖栧悎鐗�锛岄�氶亷灏嶅悗鑰呯殑鍒嗘瀽妾㈡脯閬�(d谩)鍒板皪鐩(bi膩o)鍖栧悎鐗╅��(j矛n)琛屽畾鎬у拰锛堟垨锛夊畾閲忓垎鏋愮殑鐩殑锛岄�欓爡(xi脿ng)鎶�琛�(sh霉)鍦ㄨ壊璀滃垎鏋愪腑寰楀埌浜嗗唬娉涚殑鎳�(y墨ng)鐢�銆�
琛嶇敓鍖栬│鍔戝湪琛嶇敓鍖栨妧琛�(sh霉)涓捣钁楄嚦闂�(gu膩n)閲嶈鐨勪綔鐢紝甯哥敤鐨勮鐢熷寲瑭﹀姂鏈夛細纭呯兎鍖栬│鍔�銆佺兎鍩哄寲瑭﹀姂銆�?锛涱姮顖夊櫗?銆�
鐧鹃潏濞佽鐢熷寲瑭﹀姂鐨勫劒(y艒u)鍕細
- 楂樼磾搴�---淇濊瓑琛嶇敓鍖栫敘(ch菐n)鐗╁柈涓�锛岀劇鍓敘(ch菐n)鐗�
- 鍝佺ó澶�---婊胯冻鍩虹(ch菙)鑸囨噳(y墨ng)鐢ㄧ爺绌剁殑闇�姹�
- 澶氱ó鍙嶆噳(y墨ng)楂旂郴---鍙嶆噳(y墨ng)姊濅欢婧拰锛岃鐢熷寲鍙嶆噳(y墨ng)鍙繀閫熴�佸畾閲忓湴閫�(j矛n)琛�
鈻� 纭呯兎鍖栬│鍔�
鐢茬鐑峰熀鍖栧悎鐗╂槸鏈�甯哥敤鐨勫寲瀛�(xu茅)琛嶇敓瑭﹀姂锛岀壒鍒ユ槸灏嶆埃鐩歌壊璀滆�岃█銆傜敳纭呯兎鍩鸿鐢熺墿鐨勭敓鎴愰渶瑕佹椿鎬ф矮锛堝弮鑸囧弽鎳�(y墨ng)锛燂級锛屽閰�銆侀唶椤炪�佺～閱�銆佽兒銆佹皑鍩哄寲鍚堢墿銆侀叜鍜岄啗涓殑姘紝瑭叉矮鏈冭涓夌敳鍩虹鐑烽叝鎴栦笁涓佸熀浜岀敳鍩虹鐑峰彇浠�銆�
BSTFA琛嶇敓鍖栭珨绯�
- 鍙敤浜庨仼鍚圔SA鐨勫悓椤炲寲鍚堢墿锛屽苟鐢熸垚鐩稿悓鐨勮鐢熺墿
- 鑸嘊SA鐒℃盁琛嶇敓鐗╃浉姣�锛屽彲澧炲姞鍙嶆噳(y墨ng)鍓敘(ch菐n)鐗╃殑鎻櫦(f膩)鎬�
- 涓夌敳鍩烘隘纭呯兎锛圱MCS锛夎娣诲姞鍒拌鐢熷寲閰拌兒涓�锛岃ū澶氫徊鑳哄拰鍙楀埌绌洪枔闃荤鐨勭茎鍩轰笉鏈冭垏BSTFA鍠崹(d煤)鐧�(f膩)鐢熷弽鎳�(y墨ng)
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鐢�(ch菐n)鍝佺法铏�
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绺
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鐢�(ch菐n)鍝佸悕绋�
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CAS
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鍖呰
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BSTFA
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N,O-闆�(涓夌敳鍩虹鐑峰熀)涓夋盁鐢插熀涔欓叞鑳�
N,O-Bis(trimethylsilyl)trifluoroacetamide, 98%
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25 g
100 g
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TMCS
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涓夌敳鍩烘隘纭呯兎
Chlorotrimethylsilane, 99%
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50 mL
500 mL
1 L
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BSTFA+TMCS-纭呯兎鍖栬│鍔� 99:1
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N/A
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5 mL
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MSTFA琛嶇敓鍖栭珨绯�
- 涓夌敳鍩虹鐑峰姞鍚堢墿鍏锋湁鑸嘊SA鍜孊STFA鐩稿悓鐨勭郸浜堝挤(qi谩ng)搴�
- TMCS琛嶇敓鐗╁ぇ閮ㄥ垎閮芥槸鍙彯鐧�(f膩)
- TMCS娣诲姞鍔戞湁鍔╀簬閰拌兒锛屼徊鑳哄拰鍙楅樆缇ュ熀鐨勮鐢熷寲
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鐢�(ch菐n)鍝佺法铏�
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绺
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CAS
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鍖呰
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MSTFA
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N-鐢插熀-N-(涓夌敳鍩虹鐑峰熀)涓夋盁涔欓叞鑳�
N-Methyl-N-(trimethylsilyl)trifluoroacetamide, 97%
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25 g
100 g
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TMCS
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涓夌敳鍩烘隘纭呯兎
Chlorotrimethylsilane, 99%
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50 mL
500 mL
1 L
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MTBSTFA琛嶇敓鍖栭珨绯�
- 鍙敤浜庣茎鍩�銆佺晶鍩恒�佺～閱�銆佷集鑳哄拰浠茶兒鐨勮鐢熷寲鍙嶆噳(y墨ng)
- 鍙嶆噳(y墨ng)鍓敘(ch菐n)鐗╃偤涓�т笖鏄撴彯鐧�(f膩)
- 灏嶈鐢熷彈闃荤殑閱囬鍜岃兒椤炲寲鍚堢墿锛孴BDMCS娣诲姞鍔戝彲澧炲姞瑭茶鐢熷寲瑭﹀姂鐨勭鐑峰寲鑳藉姏
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鐢�(ch菐n)鍝佺法铏�
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绺
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CAS
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鍖呰
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MTBSTFA
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N-(鍙斾竵鍩轰簩鐢茬鐑峰熀)-N-鐢插熀涓夋盁涔欓叞鑳�
N-tert-Butyldimethylsilyl-N-methyltrifluoroacetamide, 97%
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1 g
5 g
25 g
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TBDMCS
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鍙斾竵鍩轰簩鐢插熀姘鐑�
tert-Butyldimethylchlorosilane, 99%
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5 g
100 g
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鍏朵粬纭呯兎鍖栫敘(ch菐n)鍝佸垪琛�
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鐢�(ch菐n)鍝佺法铏�
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绺
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CAS
|
鍖呰
|
|
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BSA
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N,O-闆�(涓夌敳鍩虹鍩�)涔欓叞鑳�
N,O-Bis(trimethylsilyl)acetamide, 95%
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|
25 g
100 g
|
|
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DMDCS
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浜岀敳鍩轰簩姘鐑�
Dichlorodimethylsilane, 99%
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250 mL
1 L
4 L
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|
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HMDS
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鍏敳鍩轰簩纭呮爱鐑�
Hexamethyldisilazane, 98%
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25 mL
100 mL
500 mL
|
|
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TFA
|
涓夋盁涔欓吀
Trifluoroacetic acid, 99.9%
|
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250 mL
500 mL
1 L
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TMSDEA
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N-涓夌敳鍩虹鍩轰簩涔欒兒
N,N-Diethyltrimethylsilylamine, 97%
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25 g
100 g
|
|
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TMSI
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N-涓夌敳鍩虹鐑峰挭鍞�
N-Trimethylsilylimidazole, 98%
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5 g
25 g
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鈻� 鐑峰熀鍖栬│鍔�
- 鐢ㄤ簬GC鍒嗘瀽涓反姣斿Ε椤為幃(zh猫n)闈滃姂銆侀粌鍢屽懁鍜岀敓鐗╁牽绛夊寲鍚堢墿鐨勭敳鍩哄寲
- 鍖栧悎鐗╃殑琛嶇敓鍙湪姘ｇ浉鑹茶瓬鏌遍��(j矛n)妯ｅ櫒涓畬鎴�
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鐢�(ch菐n)鍝佺法铏�
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绺
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CAS
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鍖呰
|
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DMF-DEA
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N,N-浜岀敳鍩虹敳閰拌兒浜岀敳鍩虹府閱�
N,N-Dimethylformamide dimethyl acetal, 95%
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25 g
100 g
500 g
|
|
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DMF-DMA
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N,N-浜岀敳鍩虹敳閰拌兒浜屼笝鍩轰箼绺啗
N,N-Dimethylformamide dipropyl acetal, 98%
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5 g
25 g
|
|
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DMP
|
2,2-浜岀敳姘у熀涓欑兎
2,2-Dimethoxypropane, 98%
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100 mL
500 mL
1 L
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PFBBr
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α-婧�-2,3,4,5,6-浜旀盁鐢茶嫰
α-Bromo-2,3,4,5,6-pentafluorotoluene, 98%
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5 g
25 g
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NBB
|
涓佸熀纭奸吀
n-Butylboronic acid, 98%
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1 g
5 g
25 g
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TMPAH
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涓夌敳鍩鸿嫰鍩烘矮姘у寲閵�
Phenyltrimethylammonium hydroxide [20-25% solution in methanol]
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100 g
500 g
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鈻� 閰板熀鍖栬│鍔�
- 鏄撲簬鑸囬唶銆侀厷鍜岃兒椤炵墿璩�(zh矛)鐧�(f膩)鐢熷弽鎳�(y墨ng)鐢熸垚绌�(w臎n)瀹氱殑鏄撴埃鍖栬鐢熺墿锛屽彲鐢═CD銆丗ID銆丒CD鍜屽叾瀹冩娓櫒閫�(j矛n)琛屾娓�
- 鎵�鏈夌殑鍏ㄦ盁閰搁厫閮藉叿鏈夊弽鎳�(y墨ng)娲绘��
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绺
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CAS
|
鍖呰
|
|
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HFBA
|
涓冩盁涓侀吀閰�
Heptafluorobutyric anhydride, 98%
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|
5 g
25 g
|
|
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PFPA
|
浜旀盁涓欓吀閰�
Pentafluoropropionic anhydride, 98%
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|
5 g
25 g
|
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TFAA
|
涓夋盁涔欓吀閰�
Trifluoroacetic anhydride, 99%
|
|
25 g
250 g
500 g
|
|
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TFAI
|
涓欓吀閰�
Propionic anhydride, 99.5%
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500 mL
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